Fusion Materials - Design & Build a Tensile Magnetic System

This project, forming part of my MSc at the University of Bristol, gave me the opportunity to utilise my engineering experience to design and perform tensile tests on P-91 Steel, Stainless Steel & Inconel 718 alloys, to measure their suitability in upcoming national fusion programmes. This opportunity took place over the course of several months, and ended with a written dissertation, submitted to the University of Bristol, outlining my projects concept, design, methodology, results and conclusions. Throughout this page I have highlighted some of the key aspects, including background information on the project, how the test was designed and the subsequent results. Photos were taken during the process and thanks must be awarded to my professor and supervisor: Professor Mahmoud Mostafavi & Mehdi Mokhtarishirazabad.

Test Design

Figure 1. Two display cases containing 8 prepared samples of P-91 steel, having already undergone the primer coating phase of preparation these samples are ready for testing.

Figure 2. The samples were rotated in this spinning hand drill, to provide accuracy when using the dental floss to etch the two small notches into the primer.

The samples of P-91 steel, shown in Figure 1, were to be used in a Phoenix Tensile Testing Bench (provided by the University of Bristol), the preparation of the samples was as follows:

  1. Samples of P-91 steel are painted with a white VHT primer,

  2. Check the finish under the Optimax microscope

  3. Use a calliper was to create two small notches into the paint with a distance of 4.5mm Figure 2.

  4. The sample was inserted it into the tensile machine without further adjustments.

  5. After the tensile sample has been installed, the video extensometer is positioned correctly, with the light box and camera turned on

  6. Then using a black gel pen I create two straight black lines on the sample at the notches

  7. Once the lines are drawn the video extensometer is used to check the quality of the ink and if a reasonable measurement can be taken the sample is used

  8. If however, the video extensometer does not pick up the change in grey scale accurately, the sample is removed from the tensile testing rig and taken back to the preparation zone for a second attempt.

Testing Equipment

Figure 3. The Halback Magnetic Array designed to create a magnetic field perpendicular to the test sample.

Figure 4. The Phoenix Tensile Testing Bench, with the assembled camera for capturing the failure of the P-91 sample.

Test Procedure

1. Hydraulics were warmed up using the Phoenix test bench by performing load free (displacement controlled) oscillation for 5 minutes.

2. Once warming up of the hydraulics had been completed, the loadcell was zeroed and the sample was mounted.

3. If the test had a magnetic field applied to the sample, the magnet at this stage would be lifted by the student and fixed in place by the tightening of metal grips on four support poles placed through the magnet. Creating an up and down axis of movement for the magnet. (If conducted without magnet this step was ignored.).

4. The Video Extensometer was positioned, the LED light was powered on.

5. Calibrated template for the using of lens was opened in the Video Extensometer PC, marks were located and the VE measurement was engaged. This recorded both images and data.

6. Load and displacement data were synced with the VE program, the sample extension, load and crosshead displacement were recorded in one fie on the Video Extensometer PC.

7. After the sample failed or reached a recorded total load value of 35 percent maximum load, the test was stopped.

8. Video Extensometer light was turned off and the VE returned to its position on the side of the rig.

9. Load on the sample was reduced to zero using loadcell software.

10. Sample was removed from the rig.

11. Hydraulic system was turned off.

Inconel Results

Figure 5. 5 samples of Inconel tested, two with no magnet present and three with a magnet present.

Table 1. Ultimate Tensile Strength calculations for Inconel samples, averaging the maximum stress each sample endured and calculating the percentage difference.

Figure 5 is a graphical representation of the five tensile tests conducted on Inconel, two of which had no magnetic field present and three which did. They are noted by the dotted line and (M) for the magnetic tests and the dashed line and (NM) for the non-magnetic tests. Due to concerns with the time taken for each tensile test to complete to the point of necking and breaking, the five Inconel tests are of differing length, denoted by the difference in their final strain value.

It should be noted from this graphical representation that Inconel Test 1 (NM) suffered from a error with the Video Extensometer software, leading to a misreading on the two marks and subsequent loss of the extension. With the loss of reliant extension data the hydraulic rig was stopped, the load reduced to 0 and the sample removed.

The average Ultimate Tensile Strength, which is defined as the maximum stress that a material can withstand while being stretched or pulled before breaking, is recorded for the Inconel samples both with and without a magnet present in Table 1. Unlike the graphical represent of Figure 5, the mathematical average allows for an easier deduction of the difference the magnetic field has on the material properties of the Inconel. With a noted reduction in UTS of 6% between non-magnetic and magnetic testing it can be argued that the presence of the magnetic field has reduced the structural suitability of Inconel.

Stainless Steel Results

Table 2. Ultimate Tensile Strength calculations for Stainless Steel samples, averaging the maximum stress each sample endured and calculating the percentage difference.

Figure 6. All 12 samples of Stainless Steel tested, 7 with no magnet present and 5 with a magnet present.

With a larger sample size for stainless steel compared with P91 and Inconel, the results are represented in Figure 6. Figure 6, which represents the non-magnetic tensile tests Stress vs Strain, has an anomaly of (Stainless Steel Test 4 (NM)) which can be attributed to a failure to properly record the initial load (kN) and displacement (mm) the sample was undergoing due to the Phoenix Tensile rigs clamps before the actual tensile test had begun. This data set has been omitted from further manipulation.

Table 2. Displays the UTS values for the stainless steel non-magnetic and magnetic tests with the 4th test omitted due to reasons stated previously, shows a small increase in percentage difference. With a higher UTS for samples with the magnetic field present.

P-91 Steel Results

Figure 7. Five samples of P91 Steel tested, two with no magnet present and three with a magnet present

Table 3. Ultimate Tensile Strength calculations for P91 samples, averaging the maximum stress each sample endured and calculating the percentage difference

Similarly to the results shown in Figure 5, the P91 steel material had 5 available samples for use in this experiment. Figure 7, 2 for non-magnetic testing, and 3 for magnetic testing. The negative starting values for the samples can be explained by possible incorrect recordings for the displacement caused by loaded tension by the Phoenix testing rig.

This is another example of the human error that has effected the sample, and with a larger data set these risks would be mitigated. Table 3. displays a noticed drop in UTS when a magnetic field is induced perpendicular to the loading direction of the sample. Giving possible direction of a change in material properties that may make P91 steel less suitable for use in plasma confinement chambers due to the presence of a strong magnet field.

Conclusion

Despite this project developing several issues in the early stages of planning, including the limited supply of Inconel, the issues with manufacturing the Inconel samples correctly and the problems with the finish on the P91 steel samples reducing students ability to properly prepare the samples for use with the Video Extensometer. All of which contributed to the reduced scope from: Non-magnetic and magnetic tensile and creep tests at both high and room temperature on 15 samples of P91 Steel and 31 of Inconel 718. To a non-magnetic and magnetic tensile tests at room temperature on 5 samples of P91 Steel and Inconel 718 with additional tests on Stainless Steel 316. The results delivered were in support of the findings from the referenced document . The reduced ultimate tensile strength of 2.31% for P91 steel and 6.38% for Inconel 718 provide ample evidence for the need to continue research in this field to understand the micro-structural changes occurring in the metals when in the presence of a magnetic field. Understanding these changes will help us better assess the suitability of the metals for use in fusion reactor plasma confinement chambers.